AssayIndex

QSC-2412-W7745

Kisspeptin-10 · 10 mg declared · Qingdao Sigma Chemical Co., Ltd. · manufactured 06 Dec 2024

CHARACTERISEDSHARED BULK
Lot code
QSC-2412-W7745
Supplier
QSC — Qingdao Sigma Chemical Co., Ltd.
Compound
Kisspeptin-10
Compound class
Melanocortin-receptor peptides
Declared label claim
10mg
Manufacture date
06 Dec 2024
Index quarter
2025-Q1
Independent assays
5
Laboratories involved
Nordanalyt, VendorInvestigate, PeptideMeter, Medutest
Provenance mix
Buyer-sourced ×5
Section 1

Reproducibility across independent tests

Every report below is an observation of the same physical material. What they disagree about is measurement; what they agree about is the lot. The size of the disagreement is compared against what the contributing laboratories' own repeatability figures predict.

Independent assays 5
Median purity 99.72% n=5
Spread (max − min) 0.35pp n=5
Standard deviation 0.128pp n=5
97.898.298.698.999.399.7100.1This lot (QSC-2412-W7745)This lot (QSC-2412-W7745): Q1 99.68, median 99.72, Q3 99.75, n=5outlier 99.93n=5All Kisspeptin-10All Kisspeptin-10: Q1 99.13, median 99.62, Q3 99.88, n=79outlier 97.94n=79 Purity (% area)
Figure 1. This lot's independent purity results against the whole Kisspeptin-10 record set in the index. The vertical line is the index acceptance specification for the melanocortin-receptor peptides class, 98.5 % area. A narrow box on the top row against a wide box on the bottom row is the ideal reading: it means the disagreement between lots is much larger than the disagreement within this one.
Section 2

Member reports 5

Every report the index holds on this lot. Each is a page carrying its own chromatogram, mass spectrum, mass balance, provenance and caveats.

ReportLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2025-018780QSC-2412-W7745Nordanalyt2025-Q199.935.44104.3Buyer-sourced1MARGINAL
AX-2025-018781QSC-2412-W7745VendorInvestigate2025-Q199.685.17106.0Buyer-sourced1MARGINAL
AX-2025-018782QSC-2412-W7745PeptideMeter2025-Q199.585.58Buyer-sourced1MARGINAL
AX-2025-018783QSC-2412-W7745PeptideMeter2025-Q199.724.70Buyer-sourced1MARGINAL
AX-2025-018784QSC-2412-W7745Medutest2025-Q199.755.61101.7Buyer-sourced1MARGINAL
Section 3

By laboratory

Where more than one laboratory assayed this lot, the difference between them is a paired observation of their relative bias — the same material, the same time window, different instruments. Those pairs are what the index's bias estimates are built from.

LaboratoryReportsPurity results (% area)MedianGradientPublished bias (pp)Bias-adjusted
Nordanalyt199.9399.9335min+0.0299.91
VendorInvestigate199.6899.6832min-0.1199.79
PeptideMeter299.58, 99.7299.6528min-0.0599.70
Medutest199.7599.7525min+0.0899.67

This lot contributes 6 paired comparisons to the inter-lab analysis.

Section 4

The supplier's certificate for this lot

One number the supplier wrote, beside the median of the numbers other people measured on the same physical material. That comparison is only available because the index groups by lot.

FigureSupplier COAThis reportIndex note
Purity (% area)99.5999.93divergence -0.13 pp vs batch median
Total impurities (% area)not stated0.07
Largest single impurity (% area)not stated0.04
Water (%)5.15.44
Counter-ion (%)4.24.03
Peptide content (%w/w)90.190.20
Endotoxin (EU/mg)0.46not determined
Method stated on certificateYEScolumn, gradient and wavelength given
Section 5

Impurity fingerprint

The named impurities reported across this lot's assays, with how consistently each was seen. A fingerprint is what allows two lot numbers held by different companies to be identified as one bulk.

Named impurityReported inMedian % areaRange
des-Tyr (−163 Da)5 / 50.170.04–0.20
oxidised Trp (+16 Da)5 / 50.030.01–0.13
[D-Trp]-epimer4 / 50.060.02–0.09
C-terminal free acid (+1 Da)4 / 50.030.02–0.05
Section 6

Shared-bulk links

Rule AX-R09. Where impurity fingerprints and latent composition match across companies, the index treats the material as one bulk and counts it once in aggregates.

LotSold byRoleReportsMedian purity
SWB-2603-D7163SWBlinked child899.66
QSC-2412-W7745QSCthis lot599.72
Section 7

What this rollup does not establish