AX-2026-041418
GHRP-2 · 2 mg declared · Wuhan Wansheng Biotechnology Co., Ltd. · lot WWB-2511-K4194
- Report ID
- AX-2026-041418
- Compound
- GHRP-2
- Compound class
- Growth-hormone axis peptides
- Supplier
- WWB — Wuhan Wansheng Biotechnology Co., Ltd.
- Batch / lot
- WWB-2511-K4194
- Declared label claim
- 2mg
- Laboratory
- Kestrel Bioanalytical
- Assay date
- 25 Feb 2026
- Submitted
- 15 Mar 2026
- Quarter
- 2026-Q1
- Submitter
- a.petrescu
- Sample provenance
- Supplier-supplied
Results
Measured against the index acceptance specification for the growth-hormone axis peptides class. A specification is a decision the index made; a result is a measurement. See where each threshold came from.
| Parameter | Method | Result | Unit | Index spec | |
|---|---|---|---|---|---|
| Purity | RP-HPLC, 15 min gradient, 214 nm | 99.93 | % area | ≥ 99.0 | PASS |
| Total impurities | RP-HPLC, sum of reported peaks | 0.07 | % area | ≤ 1.0 | PASS |
| Largest single impurity | RP-HPLC — oxidised Trp (+16 Da) | 0.05 | % area | ≤ 1.00 | PASS |
| Identity | not ordered on this submission | not determined | — | required for VERIFIED status | NOT TESTED |
| Total peptide content | by difference from the gravimetric mass balance | 89.32 | %w/w | — | NOT TESTED |
| Target-compound content | total peptide content × purity | 89.26 | %w/w | — | NOT TESTED |
| Gross fill (as weighed) | five-place balance, under nitrogen | 2.06 | mg | 2 mg declared | NOT TESTED |
| Recovered target peptide | gross fill × target content | 1.839 | mg | 2 mg claim | NOT TESTED |
| Recovery against label claim | recovered ÷ claim | 92.0 | % | 90.0 – 110.0 | PASS |
| Water content | Karl Fischer, coulometric, duplicate | 4.82 | % | ≤ 9.0 | PASS |
| Counter-ion (acetate) | anion-exchange ion chromatography | 5.13 | % | ≤ 12.0 | PASS |
| Residual solvent + inorganic residue | estimated — see /methods/residual-solvents-q3c/ | 0.73 | % | — | NOT TESTED |
| Endotoxin | not ordered on this submission | not determined | — | ≤ 5.0 | NOT TESTED |
| Sterility | not ordered on this submission | not determined | — | no growth | NOT TESTED |
| Appearance | visual, diffuse light, black and white background | White lyophilised cake, intact | — | white to off-white intact cake | PASS |
| Reconstitution clarity | reconstituted per submitter procedure | Faint haze, clearing on standing | — | clear, no visible particulates | FAIL |
| pH (reconstituted, 1 mg/mL) | potentiometric, two-point calibration | 3.80 | — | 2.5 – 8.0 | PASS |
| Retention time (observed) | RP-HPLC, 15 min gradient | 4.87 | min | 4.89 ± 0.25 (normalised) | PASS |
| Peak asymmetry (10 % height) | Ph. Eur. 2.2.46 | 1.16 | — | 0.80 – 1.50 | PASS |
| Plate count, main peak | N = 5.54 (t/w½)² | 50,964 | — | ≥ 20,000 | PASS |
| Resolution to nearest impurity | vs C-terminal free acid (+1 Da) | 0.90 | — | no index criterion | REPORTED |
Chromatogram and peak integration
The figure is drawn from the table. It is not an independent illustration — if a number in the table changed, the trace would change with it.
| # | Peak | RT | Area (µV·s) | % area | Δ mass (Da) |
|---|---|---|---|---|---|
| 1 | GHRP-2 — main peak | 4.87 | 4,856,908 | 99.93 | — |
| 2 | oxidised Trp (+16 Da) | 4.69 | 2,430 | 0.05 | +15.995 |
| 3 | C-terminal free acid (+1 Da) | 4.95 | 972 | 0.02 | +0.984 |
| Closure check — purity + Σ impurities | 100.00 | CLOSES | |||
Reporting threshold 0.05 % area. Peaks below it are not reported and are therefore excluded from the total, which overstates purity by their sum — see peak integration.
Gravimetric mass balance
Water, counter-ion, residual and total peptide content are exhaustive and mutually exclusive categories. They must account for 100 % of the cake mass. The index closes this to within 0.02 pp and the build asserts it.
| Component | Determination | %w/w of cake |
|---|---|---|
| Water | Karl Fischer | 4.82 |
| Counter-ion (acetate) | ion chromatography | 5.13 |
| Residual solvent + inorganic residue | estimated | 0.73 |
| Total peptide content | by difference | 89.32 |
| Total | 100.00 CLOSES | |
Supplier certificate, as declared
The supplier's own figures for this lot, beside the independent measurement. Divergence is assessed against the batch median, not against this single report — see rule AX-R05.
| Figure | Supplier COA | This report | Index note |
|---|---|---|---|
| Purity (% area) | 99.90 | 99.93 | divergence +0.15 pp vs batch median |
| Total impurities (% area) | 0.10 | 0.07 | |
| Largest single impurity (% area) | 0.07 | 0.05 | |
| Water (%) | 3.7 | 4.82 | |
| Counter-ion (%) | 7.6 | 5.13 | |
| Peptide content (%w/w) | 88.1 | 89.32 | |
| Endotoxin (EU/mg) | 0.40 | not determined | |
| Method stated on certificate | YES | — | column, gradient and wavelength given |
Provenance and caveats
Where a sample came from changes the weight of the evidence. The index treats it as a first-class field.
- Sample provenance
- Supplier-supplied
- Evidentiary weight
- Weaker evidence. Read with the caveat below.
- Chain of custody
- Supplier despatch → laboratory direct (courier, cold pack, 7 d) → assay. Submitter did not handle the vial.
- Assay date
- 25 Feb 2026
- Submitted to the index
- 15 Mar 2026
- Laboratory
- Kestrel Bioanalytical, Melbourne, Australia
- Method basis
- 15 min gradient · unit-resolution MS
- Verification status
- PURITY ONLY
Annotations
No annotations on this record. Annotations are short signed technical comments from index contributors; see how to contribute.
Related records
Same batch — lot WWB-2511-K4194 n=6
| Report | Lot | Lab | Quarter | Purity % | Water % | Recovery % | Provenance | Flags | Result |
|---|---|---|---|---|---|---|---|---|---|
| AX-2026-041419 | WWB-2511-K4194 | Medutest | 2026-Q1 | 99.69 | 4.13 | — | Supplier-supplied | 1 | MARGINAL |
| AX-2026-041420 | WWB-2511-K4194 | Nordanalyt | 2026-Q1 | 99.51 | 4.94 | — | Supplier-supplied | 1 | MARGINAL |
| AX-2026-041421 | WWB-2511-K4194 | Nordanalyt | 2026-Q1 | 99.87 | 4.54 | 91.0 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-041422 | WWB-2511-K4194 | PeptideMeter | 2026-Q1 | 99.77 | 4.83 | 93.7 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-041423 | WWB-2511-K4194 | Janoshik | 2026-Q1 | 99.73 | 4.87 | 98.7 | Supplier-supplied | 1 | MARGINAL |
Cross-sections
- All GHRP-2 records n=97
- All WWB records n=522
- All Kestrel records n=404
- All 2026-Q1 records n=832
- GHRP-2 by supplier
- GHRP-2 impurity profile
| Report | Supplier | Lot | Lab | Quarter | Purity % | Water % | Recovery % | Provenance | Flags | Result |
|---|---|---|---|---|---|---|---|---|---|---|
| AX-2026-042161 | Homopeptide | HOMO-2602-E9033 | Medutest | 2026-Q2 | 99.93 | 3.99 | 105.6 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042302 | HJ | HJ-2602-W3148 | PeptideMeter | 2026-Q2 | 99.55 | 1.32 | 104.9 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042159 | Homopeptide | HOMO-2602-E9033 | Janoshik | 2026-Q2 | 99.39 | 3.77 | — | Laboratory-retained | 1 | MARGINAL |
| AX-2026-042303 | HJ | HJ-2602-W3148 | PeptideMeter | 2026-Q2 | 99.12 | 1.24 | 98.0 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042160 | Homopeptide | HOMO-2602-E9033 | Medutest | 2026-Q2 | 99.62 | 4.50 | 99.5 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-043489 | WXT | WXT-2605-U5824 | PeptideMeter | 2026-Q2 | 98.83 | 5.76 | 96.6 | Supplier-supplied | 2 | FAIL |
| AX-2026-042157 | Homopeptide | HOMO-2602-E9033 | PeptideMeter | 2026-Q2 | 99.93 | 4.32 | — | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042158 | Homopeptide | HOMO-2602-E9033 | Janoshik | 2026-Q2 | 99.59 | 4.35 | 89.8 | Buyer-sourced | 2 | MARGINAL |
| Report | Compound | Lot | Lab | Quarter | Purity % | Water % | Recovery % | Provenance | Flags | Result |
|---|---|---|---|---|---|---|---|---|---|---|
| AX-2026-041275 | Liraglutide | WWB-2607-X2189 | Nordanalyt | 2026-Q3 | 99.61 | 5.03 | 97.3 | Supplier-supplied | 0 | PASS |
| AX-2026-041387 | BPC-157 | WWB-2606-H3906 | Janoshik | 2026-Q3 | 98.95 | 4.64 | — | Laboratory-retained | 1 | MARGINAL |
| AX-2026-041334 | Semaglutide | WWB-2606-N3192 | Janoshik | 2026-Q3 | 98.83 | 5.04 | — | Supplier-supplied | 1 | MARGINAL |
| AX-2026-041337 | Semaglutide | WWB-2606-N3192 | Nordanalyt | 2026-Q3 | 98.96 | 4.81 | — | Supplier-supplied | 1 | MARGINAL |
| AX-2026-041385 | BPC-157 | WWB-2606-H3906 | Medutest | 2026-Q3 | 99.31 | 4.31 | — | Supplier-supplied | 1 | MARGINAL |
| AX-2026-041390 | BPC-157 | WWB-2606-H3906 | Medutest | 2026-Q3 | 99.47 | 4.84 | 99.3 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-041386 | BPC-157 | WWB-2606-H3906 | VendorInvestigate | 2026-Q3 | 99.32 | 4.88 | 99.2 | Buyer-sourced | 1 | MARGINAL |
| AX-2026-041335 | Semaglutide | WWB-2606-N3192 | Janoshik | 2026-Q3 | 99.55 | 4.55 | 100.5 | Supplier-supplied | 1 | MARGINAL |