AssayIndex

WXT-2411-G3549

GHRP-6 · 2 mg declared · WuXi TIDES (WuXi AppTec Testing Division) · manufactured 28 Nov 2024

CHARACTERISED
Lot code
WXT-2411-G3549
Supplier
WXT — WuXi TIDES (WuXi AppTec Testing Division)
Compound
GHRP-6
Compound class
Growth-hormone axis peptides
Declared label claim
2mg
Manufacture date
28 Nov 2024
Index quarter
2024-Q4
Independent assays
10
Laboratories involved
Janoshik, Nordanalyt, Kestrel, PeptideMeter
Provenance mix
Buyer-sourced ×1 · Supplier-supplied ×9
Section 1

Reproducibility across independent tests

Every report below is an observation of the same physical material. What they disagree about is measurement; what they agree about is the lot. The size of the disagreement is compared against what the contributing laboratories' own repeatability figures predict.

Independent assays 10
Median purity 98.96% n=10
Spread (max − min) 1.20pp n=10
Standard deviation 0.360pp n=10
97.898.198.598.999.399.7100.1This lot (WXT-2411-G3549)This lot (WXT-2411-G3549): Q1 98.82, median 98.95, Q3 99.18, n=10outlier 98.28n=10All GHRP-6All GHRP-6: Q1 99.15, median 99.65, Q3 99.93, n=169outlier 97.92n=169 Purity (% area)
Figure 1. This lot's independent purity results against the whole GHRP-6 record set in the index. The vertical line is the index acceptance specification for the growth-hormone axis peptides class, 99.0 % area. A narrow box on the top row against a wide box on the bottom row is the ideal reading: it means the disagreement between lots is much larger than the disagreement within this one.
Section 2

Member reports 10

Every report the index holds on this lot. Each is a page carrying its own chromatogram, mass spectrum, mass balance, provenance and caveats.

ReportLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2024-005394WXT-2411-G3549Janoshik2024-Q499.073.4790.6Supplier-supplied2MARGINAL
AX-2024-005395WXT-2411-G3549Janoshik2024-Q499.263.6888.8Supplier-supplied3MARGINAL
AX-2024-005396WXT-2411-G3549Nordanalyt2024-Q498.973.15Supplier-supplied3FAIL
AX-2025-021004WXT-2411-G3549Janoshik2024-Q499.483.5890.5Supplier-supplied2MARGINAL
AX-2024-005397WXT-2411-G3549Kestrel2024-Q498.283.2597.1Buyer-sourced2FAIL
AX-2024-005398WXT-2411-G3549PeptideMeter2024-Q498.833.29Supplier-supplied2FAIL
AX-2025-021005WXT-2411-G3549Nordanalyt2024-Q498.943.4689.4Supplier-supplied3FAIL
AX-2025-021006WXT-2411-G3549Janoshik2024-Q498.483.1089.1Supplier-supplied3FAIL
AX-2024-005399WXT-2411-G3549Nordanalyt2024-Q499.223.23Supplier-supplied2MARGINAL
AX-2024-005400WXT-2411-G3549Janoshik2024-Q498.823.36101.6Supplier-supplied2FAIL
Section 3

By laboratory

Where more than one laboratory assayed this lot, the difference between them is a paired observation of their relative bias — the same material, the same time window, different instruments. Those pairs are what the index's bias estimates are built from.

LaboratoryReportsPurity results (% area)MedianGradientPublished bias (pp)Bias-adjusted
Janoshik599.07, 99.26, 99.48, 98.48, 98.8299.0730min+0.0099.07
Nordanalyt398.97, 98.94, 99.2298.9735min+0.0298.95
Kestrel198.2898.2815min+0.2498.04
PeptideMeter198.8398.8328min-0.0598.88

This lot contributes 6 paired comparisons to the inter-lab analysis.

Section 4

The supplier's certificate for this lot

One number the supplier wrote, beside the median of the numbers other people measured on the same physical material. That comparison is only available because the index groups by lot.

FigureSupplier COAThis reportIndex note
Purity (% area)99.0399.07divergence +0.07 pp vs batch median
Total impurities (% area)0.970.93
Largest single impurity (% area)not stated0.46
Water (%)1.93.47
Counter-ion (%)not stated5.01
Peptide content (%w/w)93.391.03
Endotoxin (EU/mg)0.370.35
Method stated on certificateNOno method section — the result cannot be reconciled against any other
Section 5

Impurity fingerprint

The named impurities reported across this lot's assays, with how consistently each was seen. A fingerprint is what allows two lot numbers held by different companies to be identified as one bulk.

Named impurityReported inMedian % areaRange
oxidised Trp (+16 Da)10 / 100.350.11–0.84
des-Lys (−128 Da)10 / 100.180.06–0.45
[D-Trp]-epimer10 / 100.140.05–0.28
bis-oxidised Trp (+32 Da)10 / 100.220.07–0.86
Section 7

What this rollup does not establish