AssayIndex
Cross-section

GIP (1-42) impurity profile

Every named species the index has reported alongside GIP (1-42), how often, at what level, and what its presence implies about the synthesis or the handling. Reporting threshold is 0.05 % area; anything below it is invisible to this page and is silently added to the main peak.

0 recordsmedian spec 97.0 %
Named speciesΔRT (min)Δ mass (Da)Seen inMedian % areaMax % area
GIP (3-42) DPP-4 truncate (−227 Da)-0.31-227.116not observed
Met14 sulfoxide (+16 Da)-0.75+15.995not observed
deamidated (+1 Da)-0.40+0.984not observed
truncated (1-30)-2.12-1379.694not observed

Degradation pathways

Degradants are a handling finding rather than a synthesis finding. A lot that shipped clean and arrived oxidised tells you about the courier, not the chemist.

  • N-terminal Tyr-Ala cleavage by residual DPP-4 activity in impure aqueous diluent
  • Met oxidation